rac-2-{[1-(1-Adamantyl)ethyl]iminomethyl}-5-methoxyphenol
نویسندگان
چکیده
منابع مشابه
rac-2-{[1-(1-Adamantyl)ethyl]iminomethyl}-5-methoxyphenol
A novel Schiff base compound, C(20)H(27)NO(2), was obtained by a condensation of rimantadine and 2-hy-droxy-4-meth-oxy-benzaldehyde. An intra-molecular O-H⋯N hydrogen bond supports the phenol-imine tautomeric form. The adamantane and imino-methyl-4-meth-oxy-phenol units are arranged in a folded conformation [C-N-C-C torsion angle = 110.9 (3)°]. In the crystal, highly hydro-phobic adamantane moi...
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In the title compound, C(12)H(12)N(2)O(2)S, the mol-ecules have a wing-like conformation, with a distance of 3.797 (2) Å between the centroids of the five- and six-membered rings. In the crystal structure, mol-ecules are linked by N-H⋯O hydrogen bonds, forming infinite one-dimensional zigzag chains, running along [001], with a C(4) graph-set motif.
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In the racemic title compound, C14H16BrNO3S2, synthesized from the corresponding ω-bromo-propio-phenone, the dihedral angle between the plane of the phenol group and that of the planar section [maximum deviation = 0.040 (2) Å] of the morpholine-4-carbodi-thiol-ate moiety is 76.36 (10)°. A strong intra-molecular phenol O-H⋯O hydrogen bond if present in the mol-ecule. In the crystal, only weak C-...
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In the title compound, C(16)H(16)N(2)O(3)·H(2)O, the benzene rings are nearly coplanar with each other, forming a dihedral angle of 4.46 (3)°. There is a strong intra-molecular O-H⋯N hydrogen bond which results in a six-membered ring. In the crystal, the mol-ecules are connected into a three-dimensional network via O-H⋯O and O-H⋯N inter-molecular hydrogen bonds, forming a centrosymmetric ring a...
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ژورنال
عنوان ژورنال: Acta Crystallographica Section E Structure Reports Online
سال: 2011
ISSN: 1600-5368
DOI: 10.1107/s1600536811030522